3-(1-Chloroethyl)pyridine → HCID 178468822, compound

HRID 1581350Notes

Reaction equation

HRID 1581350 reaction equation
CC(Cl)c1cccnc1.N#CC1(c2cccc(C(=O)O)c2)CCOCC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1cccc(C2(C#N)CCOCC2)c1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 574410373-(4-Cyanotetrahydro-2H-pyran-4-yl)benzoic acid

Product 1

HCID 178468822HCID 178468822, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-099e91a2b016475386002b87e382cac3
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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