3-(1-Chloroethyl)pyridine → HCID 178486366, compound

HRID 1581353Notes

Reaction equation

HRID 1581353 reaction equation
CC(Cl)c1cccnc1.COc1c2ccc(C(=O)O)cc2nn1C(C)(C)C>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COc1c2ccc(C(=O)OC(C)c3cccnc3)cc2nn1C(C)(C)C

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 178486364HCID 178486364, compound

Product 1

HCID 178486366HCID 178486366, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-e578c95d5e0f406fa8166168a52817db
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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