4-Methyl-3-(morpholine-4-sulfonyl)-benzoic acid → HCID 178425905, compound

HRID 1581361Notes

Reaction equation

HRID 1581361 reaction equation
CC(Cl)c1cccnc1.Cc1ccc(C(=O)O)cc1S(=O)(=O)N1CCOCC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1ccc(C(=O)OC(C)c2cccnc2)cc1S(=O)(=O)N1CCOCC1

Participants

6

Reactant 2

HCID 7678974-Methyl-3-(morpholine-4-sulfonyl)-benzoic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178425905HCID 178425905, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-438530dd09ea42c8a0baa161121519e6
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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