3-(1-Chloroethyl)pyridine → HCID 178468738, compound

HRID 1581368Notes

Reaction equation

HRID 1581368 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1ccc(C2CCCN2)cc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1ccc(C2CCCN2)cc1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 230095054-(Pyrrolidin-2-yl)benzoic acid

Product 1

HCID 178468738HCID 178468738, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-9edcab5316084c77a2e386ba4405dc42
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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