3-(3-BROMO-PHENYL)-4,5-DIHYDRO-ISOXAZOLE-5-CARBOXYLIC ACID → HCID 178468613, compound

HRID 1581371Notes

Reaction equation

HRID 1581371 reaction equation
CC(Cl)c1cccnc1.O=C(O)C1CC(c2cccc(Br)c2)=NO1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)C1CC(c2cccc(Br)c2)=NO1)c1cccnc1

Participants

6

Reactant 2

HCID 29622523-(3-BROMO-PHENYL)-4,5-DIHYDRO-ISOXAZOLE-5-CARBOXYLIC ACIDHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178468613HCID 178468613, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-03322f3a89c84c559d2ac88510e71385
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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