3-(1-Chloroethyl)pyridine → HCID 178491338, compound

HRID 1581377Notes

Reaction equation

HRID 1581377 reaction equation
CC(Cl)c1cccnc1.COc1cccc(OC)c1C1(C(=O)O)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COc1cccc(OC)c1C1(C(=O)OC(C)c2cccnc2)CC1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 442449981-(2,6-dimethoxyphenyl)Cyclopropanecarboxylic acid

Product 1

HCID 178491338HCID 178491338, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-7fc397d0f76645d58d837e0201e8fd55
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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