3-(1-Chloroethyl)pyridine → HCID 178503230, compound

HRID 1581380Notes

Reaction equation

HRID 1581380 reaction equation
CC(Cl)c1cccnc1.CSc1ccc(C(=O)[C@H]2CCCC[C@H]2C(=O)O)cc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CSc1ccc(C(=O)[C@H]2CCCC[C@H]2C(=O)OC(C)c2cccnc2)cc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 247224202-[4-(Methylsulfanyl)benzoyl]cyclohexane-1-carboxylic acid

Product 1

HCID 178503230HCID 178503230, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-4d705a748f994c619f5b574a8db56288
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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