HCID 13422553, compound → HCID 178490795, compound

HRID 1581387Notes

Reaction equation

HRID 1581387 reaction equation
CC(Cl)c1cccnc1.COc1ccc(CN2CC(C(=O)O)CC2=O)cc1OC>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COc1ccc(CN2CC(C(=O)OC(C)c3cccnc3)CC2=O)cc1OC

Participants

6

Reactant 2

HCID 13422553HCID 13422553, compoundHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178490795HCID 178490795, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-d6163d4dfd1e48d593d15bf7fccce195
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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