3-(1-Chloroethyl)pyridine → HCID 178456308, compound

HRID 1581391Notes

Reaction equation

HRID 1581391 reaction equation
CC(Cl)c1cccnc1.CCCN1CC(C(=O)O)CCC1=O>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CCCN1CC(C(=O)OC(C)c2cccnc2)CCC1=O

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 448276896-Oxo-1-propylpiperidine-3-carboxylic acid

Product 1

HCID 178456308HCID 178456308, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-d82d57081cca43ca85d4f745be8844ec
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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