3-(1,1,3-Trioxo-1,3-dihydro-2H-1lambda~6~,2-benzothiazol-2-yl)propanoic acid → HCID 178471845, compound

HRID 1581394Notes

Reaction equation

HRID 1581394 reaction equation
CC(Cl)c1cccnc1.O=C(O)CCN1C(=O)c2ccccc2S1(=O)=O>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)CCN1C(=O)c2ccccc2S1(=O)=O)c1cccnc1

Participants

6

Reactant 2

HCID 20635863-(1,1,3-Trioxo-1,3-dihydro-2H-1lambda~6~,2-benzothiazol-2-yl)propanoic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178471845HCID 178471845, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-626f0da16c8f42f9b4d25b3ed9184921
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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