Tetrahydro-3-thiophenecarboxylic acid → HCID 178469393, compound

HRID 1581401Notes

Reaction equation

HRID 1581401 reaction equation
CC(Cl)c1cccnc1.O=C(O)C1CCSC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)C1CCSC1)c1cccnc1

Participants

6

Reactant 2

HCID 13581851Tetrahydro-3-thiophenecarboxylic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178469393HCID 178469393, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-e68a11ec234e4f4a86199a6dcab54308
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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