2-Methyloxolane-2-carboxylic acid → HCID 178468927, compound

HRID 1581403Notes

Reaction equation

HRID 1581403 reaction equation
CC(Cl)c1cccnc1.CC1(C(=O)O)CCCO1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)C1(C)CCCO1)c1cccnc1

Participants

6

Reactant 2

HCID 31643262-Methyloxolane-2-carboxylic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178468927HCID 178468927, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-db3f467481f844218f955054bee1de62
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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