3-(1-Chloroethyl)pyridine → HCID 178433543, compound

HRID 1581408Notes

Reaction equation

HRID 1581408 reaction equation
CC(Cl)c1cccnc1.Cc1nc(SC(C)(C)C(=O)O)sc1C>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1nc(SC(C)(C)C(=O)OC(C)c2cccnc2)sc1C

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 81229052HCID 81229052, compound

Product 1

HCID 178433543HCID 178433543, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-9fafc66cb4034b859a5afcd436e3c9cd
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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