3-(1-Chloroethyl)pyridine → HCID 178468408, compound

HRID 1581411Notes

Reaction equation

HRID 1581411 reaction equation
CC(Cl)c1cccnc1.CC12CC(C(=O)O)(CO1)C2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)C12COC(C)(C1)C2)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 1322611251-methyl-2-oxabicyclo[2.1.1]hexane-4-carboxylic acid

Product 1

HCID 178468408HCID 178468408, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-02eb4ac01df24ede9ffcc42beb882e70
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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