3-(1-Chloroethyl)pyridine → HCID 178458795, compound

HRID 1581414Notes

Reaction equation

HRID 1581414 reaction equation
C#CCOc1cnc(C(=O)O)cn1.CC(Cl)c1cccnc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>C#CCOc1cnc(C(=O)OC(C)c2cccnc2)cn1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 584486085-Prop-2-ynyloxypyrazine-2-carboxylic acid

Product 1

HCID 178458795HCID 178458795, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-5dcab926c9914261800b209e91bd97de
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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