3-(1-Chloroethyl)pyridine → HCID 178469461, compound

HRID 1581421Notes

Reaction equation

HRID 1581421 reaction equation
CC(Cl)c1cccnc1.CN1CCc2cc(C(=O)O)cnc21>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1cnc2c(c1)CCN2C)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 118999898HCID 118999898, compound

Product 1

HCID 178469461HCID 178469461, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-0b766171d4e442388db567f7eb5357c9
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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