3-(1-Chloroethyl)pyridine → HCID 178468694, compound

HRID 1581423Notes

Reaction equation

HRID 1581423 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1ccc2nnc(C3CC3)n2c1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1ccc2nnc(C3CC3)n2c1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 621386533-Cyclopropyl-[1,2,4]triazolo[4,3-a]pyridine-6-carboxylic acid

Product 1

HCID 178468694HCID 178468694, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-35aeb12a3a6a4f2c9264c7f70030e4ac
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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