3-(1-Chloroethyl)pyridine → HCID 178468664, compound

HRID 1581427Notes

Reaction equation

HRID 1581427 reaction equation
CC(Cl)c1cccnc1.Cn1c(=O)c2ccc(C(=O)O)nc2n(C)c1=O>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1ccc2c(=O)n(C)c(=O)n(C)c2n1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 246978541,2,3,4-Tetrahydro-1,3-dimethyl-2,4-dioxopyrido[2,3-d]pyrimidine-7-carboxylic acid

Product 1

HCID 178468664HCID 178468664, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-188d83fcd1a942f7804d4277f87ae3d3
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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