3-(1-Chloroethyl)pyridine → HCID 178468718, compound

HRID 1581428Notes

Reaction equation

HRID 1581428 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1cccc2c1OC(F)(F)C2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1cccc2c1OC(F)(F)C2)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 686086687-Benzofurancarboxylic acid, 2,2-difluoro-2,3-dihydro-

Product 1

HCID 178468718HCID 178468718, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-741a0a878e974c159e2fdf1c602888bb
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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