5-Bromobenzo(1,3)dioxole-4-carboxylic acid → HCID 178468456, compound

HRID 1581431Notes

Reaction equation

HRID 1581431 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1c(Br)ccc2c1OCO2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1c(Br)ccc2c1OCO2)c1cccnc1

Participants

6

Reactant 2

HCID 125141065-Bromobenzo(1,3)dioxole-4-carboxylic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178468456HCID 178468456, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-537ba51b732c49beb28265af590db88c
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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