1-Bromooctane → 2,7-Dibromo-9,9-di-n-octylfluorene

HRID 1581457Notes

Reaction equation

HRID 1581457 reaction equation
[Br:1][C:2]1[CH:14]=[CH:13][C:12]2[C:11]3[C:6](=[CH:7][C:8]([Br:15])=[CH:9][CH:10]=3)[CH2:5][C:4]=2[CH:3]=1.[CH2:16](Br)[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]>>[Br:1][C:2]1[CH:14]=[CH:13][C:12]2[C:11]3[C:6](=[CH:7][C:8]([Br:15])=[CH:9][CH:10]=3)[C:5]([CH2:13][CH2:14][CH2:2][CH2:3][CH2:4][CH2:12][CH2:11][CH3:10])([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 81401-BromooctaneHCID 1400732,7-Dibromofluorene

Product 1

HCID 52153212,7-Dibromo-9,9-di-n-octylfluoreneYield 85%

Procedure

This compound was prepared from 2,7-dibromofluorene and n-octyl bromide, using a similar procedure as described in Example III. The product was obtained in an 85% yield as colorless crystals.

Workup

  1. customThe product was obtained in an 85% yield as colorless crystals

Sources & evidence

ORD record
ord-339313ea8ea641e99aca8860cdb54b1b
Source dataset
uspto-grants-2004_05
Patent number
US06730417B2

Reaction notes

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