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HRID1581716

反应详情

EQUATION

反应方程式

HRID 1581716 反应方程式

REACTANTS

反应物

1
N-[2-(5-nitro-1H-indol-3-yl)ethyl]acetamide 分子结构式
HCID906605

N-[2-(5-nitro-1H-indol-3-yl)ethyl]acetamide

C12H13N3O3

PRODUCTS

产物

1
N-[2-(5-Amino-1H-indol-3-yl)ethyl]acetamide 分子结构式
HCID22722278

N-[2-(5-Amino-1H-indol-3-yl)ethyl]acetamide

C12H15N3O

AUXILIARIES

试剂、催化剂与溶剂

2
Palladium 分子结构式
催化剂HCID23938

Palladium

Pd

Ethanol 分子结构式
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The product from Example 2 (0.05 mmol) is taken into ethanol (3 mL) and hydrogenated 6 h at 3 atmospheres of H2 pressure over a catalytic amount of 10% Pd/C. The catalyst is removed by filtration through Celite and the solvent removed in vacuo, affording the title compound. This product is somewhat air sensitive and is used immediately for subsequent reactions.

WORKUP

后处理

  1. customThe catalyst is removed by filtration through Celite
  2. customthe solvent removed in vacuo