HRID1582014

反应详情

EQUATION

反应方程式

HRID 1582014 的结构方程式

PROCEDURE

实验过程

Using 4-hydroxythieno[3,2-d]pyrimidine (60 mg, 0.39 mmol), and phosphorus oxychloride (0.6 ml), and then 2-aminoindan (210 mg, 1.56 mmol), a similar procedure to Example 5 was carried out. The product obtained was purified by silica gel chromatography (hexane:ethyl acetate=1:2) to obtain the title compound (30 mg, 0.11 mmol) having the following physical properties:

WORKUP

后处理

  1. customThe product obtained
  2. customwas purified by silica gel chromatography (hexane:ethyl acetate=1:2)