HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Carbazol-9-yl-ethoxy)-ethanol → 2-[2-(9H-Carbazole-9-yl)ethoxy]ethanol 3,4,5-tris(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Carbazol-9-yl-ethoxy)-ethanol | HCID 657489 | — |
| Reactant | 3,4,5-Tris(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyloxy)benzoic acid | HCID 11320874 | — |
| Reactant | dendron D1 | HCID 86277907 | — |
| Product | 2-[2-(9H-Carbazole-9-yl)ethoxy]ethanol 3,4,5-tris(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyloxy)benzoate | HCID 22719304 | — |
Reaction Steps
The synthesis of a mobility donor fluorinated dendron D1 of the present invention is as shown in the Scheme below. D1 is prepared using 3,4,5-tris-(12,12,12,11,11,10,10,9,9,8,8,7,7,6,6,5,5-heptadecafluoro-n-dodecan-1-yloxy)-benzoic acid as a starting material. The intermediate is then reacted with an alcohol of the desired apex moiety, 2-(2-carbazol-9yl-ethoxy)-ethanol, to obtain the compound of the invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06733883B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-85717f65ccb4413d96d4b42780f39c8c |
| Source note | uspto-grants-2004_05 |