HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 657489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Carbazole | HCID 6854 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-[2-(2-Chloroethoxy)ethoxy]oxane | HCID 10965737 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 657489 | HCID 657489 | — |
Reaction Steps
To a flask containing 100 ml benzene, 100 ml 50% NaOH, was added carbazole (2) (20 g, 0.12 mmol), 4 g benzyltriethylammonium chloride (TEBA), 1 g of NaI and 2-[2-(2-chloroethoxy)-ethoxy]-tetrahydropyran (3) (38 g, 0.12 mmol) under N2. The mixture was refluxed for 6 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06733883B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-e652bf869a7c42fea8480b94f0f85f6a |
| Source note | uspto-grants-2004_05 |