HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → 1-(6-Isopropyl-4,4-dimethyl-1-n-propyl-1,2,3,4-tetrahydro-quinolin-8-yl)-ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | 1-(6-Isopropyl-4,4-dimethyl-1-n-propyl-1,2,3,4-tetrahydro-quinolin-8-yl)-ethanol | HCID 22719821 | — |
| Product | 1-(6-Isopropyl-4,4-dimethyl-1-n-propyl-1,2,3,4-tetrahydro-quinolin-8-yl)-ethanone | HCID 22719832 | — |
Reaction Steps
Following General Procedure D, 1-(1-n-propyl-6-isopropyl-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-8-yl)-ethan-1-ol (Intermediate 11, 4.54 g, 18.1 mmol) and 4-methylmorpholine N-oxide (4.23 g, 36.2 mmol) were reacted to give the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06734193B1 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-845573d89c5f4978af956fca7b35d7fe |
| Source note | uspto-grants-2004_05 |