Sodium Formate → HCID 10659637, compound

Participants

Reaction Steps

A mixture of compound 11 (750 mg, 2.09 mmol) and 10% Pd/C (500 mg) was suspended in methanol (20 mL) and sodium formate (700 mg, 11.1 mmol) was added. The reaction was conducted at refluxing for 10 min and cooled to ambient temperature. The catalyst was filtered off and the mixture was concentrated under reduced pressure to give compound 12 (540 mg, 96%) as a white solid material.

Provenance & Evidence