HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 135476517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 137178931 | HCID 137178931 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 135476517 | HCID 135476517 | — |
Reaction Steps
To a solution of compound 22 in methanol (20 mL) was added 2M NaOH (2 mL) and 15 min later acetic acid (2 mL). The mixture was cooled in ice-bath, the precipitate was filtered off, washed with water and dried in vacuo. Yield: 0.69 g (85%) of compound 23 as a white solid material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06734291B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-c80635c0bd0a40d08d491b72c0e2d304 |
| Source note | uspto-grants-2004_05 |