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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1582433Generated: November 1, 2026

Acetic Acid → HCID 135476517, compound

https://huagongshe.com/reaction/1582433

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 137178931HCID 137178931—
SolventMethanolHCID 887—
ProductHCID 135476517HCID 135476517—

Reaction Steps

To a solution of compound 22 in methanol (20 mL) was added 2M NaOH (2 mL) and 15 min later acetic acid (2 mL). The mixture was cooled in ice-bath, the precipitate was filtered off, washed with water and dried in vacuo. Yield: 0.69 g (85%) of compound 23 as a white solid material.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06734291B2
Source datasetuspto-grants-2004_05
ORD IDord-c80635c0bd0a40d08d491b72c0e2d304
Source noteuspto-grants-2004_05