HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22717653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 69864680 | HCID 69864680 | — |
| Product | HCID 22717653 | HCID 22717653 | — |
Reaction Steps
2 g (8.2 mmol) of 9-ethyl-4-hydroxy-6,7,8,9-tetrahydro-1H-pyrido[2,3-g]quinol-2-one are suspended in 25 ml of dimethylformamide and treated with 6.7 g (0.12 mol) of potassium hydroxide. 8.6 g (0.07 mol) of dimethyl sulfate are added dropwise thereto at at most 60° C. (cooling with ice/sodium chloride bath). The suspension is discharged into 200 ml of water. A well filterable precipitate is formed, which is filtered off with suction and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06737280B1 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-bd5e7d021a9044da879d4efa5a0b8bc5 |
| Source note | uspto-grants-2004_05 |