Propane, 2,2',2''-[methylidynetris(oxy)]tris- → HCID 22717683, compound

Participants

Reaction Steps

A solution of the compound of Step A (1.0 g, 3.6 mmol) in 20 mL of triisopropylorthoformate was heated at 145° C. for 2 h and then allowed to stir at ambient temperature overnight. The volatiles were removed under reduced pressure, and the residue recrystallized from methanol to give 0.99 g (86%) of the title compound, a compound of this invention, as a solid melting at 78-80° C.

Provenance & Evidence