HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22718382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10271308 | HCID 10271308 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22718382 | HCID 22718382 | — |
Reaction Steps
1-(4-Phenylsulfonyl-2-o-tolyl-oxazol-5-yl)piperazine (0.2 g, 0.556 mmol) was dissolved in tetrahydrofuran (15 ml) and methanol (15 ml), mixed with methanolic hydrochloric acid (2 ml) at room temperature and subsequently stirred for 1 h. The precipitated crystals were filtered off with suction, washed with a small amount of tetrahydrofuran and dried in air.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06737426B1 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-42c08016b9dd4071a99d9f3c08549d64 |
| Source note | uspto-grants-2004_05 |