HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzyl chloride → 2-(5-chloro-2-((2,4-dichlorobenzyl)oxy)phenyl)-1-(1H-1-imidazolyl)-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzyl chloride | HCID 7212 | — |
| Reactant | 4-chloro-2-(1-hydroxy-2-(1H-1-imidazolyl)-1-methylethyl)phenol | HCID 12972897 | — |
| Product | 2-(5-chloro-2-((2,4-dichlorobenzyl)oxy)phenyl)-1-(1H-1-imidazolyl)-2-propanol | HCID 12972902 | 51.9% |
Reaction Steps
The general procedure of Example 6 was repeated using 4-chloro-2-(1-hydroxy-2-(1H-1-imidazolyl)-1-methylethyl)phenol [compound (2-1)] and 2,4-dichlorobenzyl chloride, to thereby yield 2-(5-chloro-2-((2,4-dichlorobenzyl)oxy)phenyl)-1-(1H-1-imidazolyl)-2-propanol as colorless crystals (yield: 51.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06737434B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-37956bfe11a14bc9b52d2a0b5d3d6048 |
| Source note | uspto-grants-2004_05 |