Ethylamine → HCID 22716716, compound

Participants

Reaction Steps

To a THF solution of 2,6-dichloro-3-(3-chlorobenzoyl)pyridine was added a 70% ethylamine aqueous solution, followed by reaction at room temperature. Thereafter, the reaction mixture was worked up and purified in a usual manner to obtain 6-chloro-3-(3-chlorobenzoyl)-2-ethylaminopyridine. NMR1: 8.95 (1H, brs), 6.48 (1H, d, J=7.8 Hz), 1.31 (3H, t, J=7.1 Hz).

Provenance & Evidence