HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Formylsalicylic acid → n,n-Di-n-pentyl-2-hydroxy-5-formylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Formylsalicylic acid | HCID 69226 | — |
| Reactant | n,n-Di-n-pentyl-2-methoxy-5-formylbenzamide | HCID 22716819 | — |
| Product | n,n-Di-n-pentyl-2-hydroxy-5-formylbenzamide | HCID 22716814 | — |
Reaction Steps
N,N-Di-n-pentyl-2-hydroxy-5-formylbenzamide was prepared from 5-formylsalicylic acid (250 mg, 1 eq) using the same procedure as for N,N-di-n-pentyl-2-methoxy-5-formylbenzamide. The product was obtained as pale brown oil (211 mg, 46%). 1H NMR (CDCl3) δ9.67 (s, 1H, O═C—H), 3.33 (m, 4H, NCH2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06740670B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-22397d92933a4153b277eb5bb498330e |
| Source note | uspto-grants-2004_05 |