HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178447925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodohexane | HCID 12527 | — |
| Reactant | HCID 178444374 | HCID 178444374 | — |
| Reactant | HCID 178444967 | HCID 178444967 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178447925 | HCID 178447925 | — |
Reaction Steps
A mixture of 28.2 g of 2,6-difluoro-4-(trans-4-pentylcyclohexyl)-phenol, 6.9 g of K2CO3, 25 g of hexyl iodide and 250 ml of dimethylformamide is heated at 80° for 16 hours, while stirring, and is then cooled and worked up in the usual manner. This gives 2,6-difluoro-4-(trans-4-pentylcyclohexyl)-1-hexoxybenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551264 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-9a326e45977b499d8783d3a34d3d445a |
| Source note | uspto-grants-1985_11 |