HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 75863-26-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 18600037 | HCID 18600037 | — |
| Product | 75863-26-2 | HCID 222847 | — |
Reaction Steps
The compound prepared in Example 9a (450 mg) was hydrolized in methylenechloride (15 ml) and diethylether (30 ml) at 20° C. for two minutes. The product obtained was purified by filtration over alumina. Yield 235 mg (75%). Crystallization from methanol gave the title product, m.p. 200°-204° C. (dec.) (alpha)22 +134 (CHCl3, c 1.00).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551278 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-6bc7793d659d4fc882945421b7432e9c |
| Source note | uspto-grants-1985_11 |