HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10882550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 18600042 | HCID 18600042 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10882550 | HCID 10882550 | — |
Reaction Steps
The title compound was prepared by hydrolysis of the compound prepared in Example 15a in a mixture of methylene chloride (5 ml) and diethyl ether (25 ml). This mixture was stirred vigorously with hydrochloric acid (2 ml, 38%), for 5 minutes. After work up and chromatography (methylene chloride, alumina act. II-III) the title compound was obtained (55 mg, 15%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551278 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-e577995731f14c20a0317dbbf094c3c4 |
| Source note | uspto-grants-1985_11 |