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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1583262Generated: November 1, 2026

Hydrochloric Acid → HCID 10882550, compound

https://huagongshe.com/reaction/1583262

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 18600042HCID 18600042—
SolventDichloromethaneHCID 6344—
ProductHCID 10882550HCID 10882550—

Reaction Steps

The title compound was prepared by hydrolysis of the compound prepared in Example 15a in a mixture of methylene chloride (5 ml) and diethyl ether (25 ml). This mixture was stirred vigorously with hydrochloric acid (2 ml, 38%), for 5 minutes. After work up and chromatography (methylene chloride, alumina act. II-III) the title compound was obtained (55 mg, 15%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04551278
Source datasetuspto-grants-1985_11
ORD IDord-e577995731f14c20a0317dbbf094c3c4
Source noteuspto-grants-1985_11