HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54197380, compound → HCID 23316677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54197380 | HCID 54197380 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23316677 | HCID 23316677 | — |
Reaction Steps
A solution of hexahydro-3,5-dioxo-1H-pyrrolizine-2-carboxylic acid benzyl ester 25.90.1 g, yy mole) in dioxane (200 ml) is treated with hydrogen gas in the presence of 20% Pd/C catalyst for eight hours. The mixture is filtered and concentrated at reduced pressure (below 25° C.) to yield pure hexahydro-3,5-dioxo-1H-pyrrolizine-2-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551470 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-1148e262ad6c441880a3014280eb46da |
| Source note | uspto-grants-1985_11 |