Hydrochloric Acid → HCID 131714406, compound

HRID 1583388Notes

Reaction equation

HRID 1583388 reaction equation
[NH2:1][C:2]1[NH:3][C:4](=[O:12])[C:5]2[N+:6]([O-:11])=[CH:7][NH:8][C:9]=2[N:10]=1.[ClH:13]>>[ClH:13].[N:3]1[C:4](=[O:12])[C:5]2[C:9]([N:8]=[CH:7][N+:6]=2[O-:11])=[N:10][C:2]=1[NH2:1]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178508254HCID 178508254, compound

Product 1

HCID 131714406HCID 131714406, compound

Procedure

2-Amino-1,9-dihydro-6H-purin-6-one-7-oxide (52.3 mg, 0.31 mmol) was heated over a steam bath in 5 ml of 1.0M aqueous hydrochloric acid until it dissolved. The solution was filtered and allowed to cool to room temperature. Upon standing, 47.3 mg of the hydrochloride salt of 2-amino-1,9-dihydro-6H-purin-6-one-7-oxide precipitated as fine, white needles, mp >250° C.

Workup

  1. dissolutiondissolved
  2. filtrationThe solution was filtered
  3. custom47.3 mg of the hydrochloride salt of 2-amino-1,9-dihydro-6H-purin-6-one-7-oxide precipitated as fine, white needles, mp >250° C.

Sources & evidence

ORD record
ord-4a1aa7d48f2147828b55638376dfcbf5
Source dataset
uspto-grants-1985_11
Patent number
US04551529

Reaction notes

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