HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13506753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 13506752 | HCID 13506752 | — |
| Solvent | Ethyl orthoformate | HCID 31214 | — |
| Product | HCID 13506753 | HCID 13506753 | — |
Reaction Steps
A 2.0 g amount of 5-(4-pyridyl)imidazo[1,2-a]pyrimidine was suspended in 100 ml of triethylorthoformate and 1.67 ml of concentrated hydrochloric acid was added. After standing at room temperature for 6 hours the resultant precipitate was collected by filtration and gave 0.47 g of the product of the Example as a yellow solid, mp 295°-300° C.(dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551530 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-80284bac25664b10bc5095acee8f668a |
| Source note | uspto-grants-1985_11 |