HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → HCID 54180870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Product | HCID 54180870 | HCID 54180870 | — |
Reaction Steps
A mixture of 40.0 g of 3-acetylpyridine and 50.0 ml of dimethylacetamide dimethylacetal was heated on a steam bath for 6 hours under argon. The volatile components were then removed in vacuo and hexane was added to the resultant thick syrup to crystallize the product. Filtration gave 33.5 g of the desired product as red-brown crystals, mp 62°-64° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551530 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-3dae5f4025444a48802a3714279c5232 |
| Source note | uspto-grants-1985_11 |