HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 20260634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Bromobutan-1-amine--hydrogen bromide (1/1) | HCID 24189510 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20260634 | HCID 20260634 | — |
Reaction Steps
A solution of 17.4 g of 4-bromobutanamine hydrobromide and 6.0 ml (5.9 g) of pyridine in 75 ml of ethanol was heated under reflux for 18 hours. The reaction was cooled and the resulting solid was collected and recrystallized from ethanol to give 3.4 g (15%) of the analytical sample as colorless crystals, 1-(4-aminobutyl)pyridinium bromide hydrobromide mp 219° (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551460 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-dc3179eb977e41668e8a54c6482d592a |
| Source note | uspto-grants-1985_11 |