HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 13535829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 1-(2,3-Dihydro-2-methylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazide | HCID 13535828 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13535829 | HCID 13535829 | — |
Reaction Steps
3.0 g of 1E was added to a stirred solution of 75 ml of 12.5% phosgene in benzene. The resulting mixture was stirred for 2 hours at room temperature, then the solvent was evaporated to give 1-(chlorocarbonyl)-1-(2,3-dihydro-2-methylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazide (1F), as an amber syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04554283 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-4d8dff9d476a411a80d54c86637d488e |
| Source note | uspto-grants-1985_11 |