Water → 5323-58-0

HRID 1583803Notes

Reaction equation

HRID 1583803 reaction equation
O.C([O:4][C:5]1[C:14]([O:15][CH3:16])=[CH:13][C:12]([N+:17]([O-:19])=[O:18])=[C:11]2[C:6]=1[CH:7]=[CH:8][CH:9]=[N:10]2)C.C(=O)(O)[O-].[Na+]>C(O)(=O)C>[OH:4][C:5]1[C:14]([O:15][CH3:16])=[CH:13][C:12]([N+:17]([O-:19])=[O:18])=[C:11]2[C:6]=1[CH:7]=[CH:8][CH:9]=[N:10]2

Participants

5

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 619159HCID 619159, compound

Product 1

HCID 1353992885323-58-0

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The water washings of the crude 5-ethoxy-6-methoxy-8-nitroquinoline were acidified with acetic acid and basified with sodium bicarbonate to give 0.44 g of 5-hydroxy-6-methoxy-8-nitroquinoline.

Sources & evidence

ORD record
ord-f9d991316656462ab8f48272bf8f59de
Source dataset
uspto-grants-1985_11
Patent number
US04554279

Reaction notes

Loading…