HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Oxazolidinedione → HCID 9888581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Oxazolidinedione | HCID 97389 | — |
| Reactant | HCID 53680384 | HCID 53680384 | — |
| Product | HCID 9888581 | HCID 9888581 | — |
Reaction Steps
In substantially the same manner as in Working Example 11, 3-fluoro-4-(5-methyl-2-phenyl-4-oxazolyl methoxy)cinnamaldehyde was condensed with 2,4-oxazolidinedione. The condensate was subjected to catalytic reduction to yield 5-[3-[3-fluoro-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propyl]-2,4-oxazolidinedione, which was recrystallized from dichloromethane-methanol to give colorless prisms, m.p.180-181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-2d018faea9114338af4dae25a37cb3bb |
| Source note | uspto-grants-1999_08 |