HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Oxazolidinedione → HCID 86754367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Oxazolidinedione | HCID 97389 | — |
| Reactant | HCID 73768319 | HCID 73768319 | — |
| Product | HCID 86754367 | HCID 86754367 | — |
Reaction Steps
In substantially the same manner as in Working Example 11, 3-fluoro-4-[2-[N-methyl-N-(2-pyridyl)amino]ethoxy]cinnamaldehyde was condensed with 2,4-oxazolidinedione. The condensate was subjected to catalytic hydrogenation to yield 5-[3-[3-fluoro-4-[2-[N-methyl-N-(2-pyridyl)amino]ethoxy]phenyl]propyl-2,4-oxazolidinedione, which was recrystallized from ethyl acetate-hexane to give colorless prisms, m.p.124-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-0f902d4db8e34d5e99ee18964381156d |
| Source note | uspto-grants-1999_08 |