HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Difluoro-4-nitrobenzene → HCID 21224468, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Difluoro-4-nitrobenzene | HCID 123053 | — |
| Reactant | 2-(N-Methyl-N-(2-pyridyl)amino)ethanol | HCID 737420 | — |
| Product | HCID 21224468 | HCID 21224468 | — |
Reaction Steps
In substantially the same manner as in Reference Example 54, 3,4-difluoronitrobenzene was reacted with 2-[N-methyl-N-(2-pyridyl)amino]ethanol to yield 3-fluoro-4-[2-[N-methyl-N-(2-pyridyl)amino]ethoxy]nitrobenzene. The product was recrystallized from ethyl acetate-hexane to give yellow prisms, m.p.95-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-aca5cc439b8b40128fc2fd4e37049b8a |
| Source note | uspto-grants-1999_08 |