HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 21224409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 69831620 | HCID 69831620 | — |
| Product | HCID 21224409 | HCID 21224409 | — |
Reaction Steps
In substantially the same manner as in Reference Example 58, methyl 3-fluoro-4-[2-[N-methyl-N-(2-pyridyl)amino]ethoxy]cinnamate was subjected to reduction reaction with diisobutylaluminum hydride to yield (E)-3-(3-fluoro-4-[2-[N-methyl-N-(2-pyridyl)amino]ethoxy]phenyl]-2-propen-1-ol. The product was recrystallized from ethyl acetate-hexane to give colorless needles, m.p.80-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-afc0805879a24a89a6df1931b40c0a07 |
| Source note | uspto-grants-1999_08 |