HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyryl chloride → HCID 22034976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Product | HCID 22034976 | HCID 22034976 | 77% |
Reaction Steps
The product is prepared analogously to Example 1 from isobutyryl chloride and aminoacetaldehyde dimethyl acetal. Distillation at 98° C. and 0.01 mbar gives a yield of 77%. According to GC, the product has a purity of 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932674 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-649a3a20f67e409fb2c4de54c66dda1c |
| Source note | uspto-grants-1999_08 |