Isobutyryl chloride → HCID 22034976, compound

HRID 1584514Notes

Reaction equation

HRID 1584514 reaction equation
[C:1](Cl)(=[O:5])[CH:2]([CH3:4])[CH3:3].[CH3:7][O:8][CH:9]([O:12][CH3:13])[CH2:10][NH2:11]>>[CH3:7][O:8][CH:9]([O:12][CH3:13])[CH2:10][NH:11][C:1](=[O:5])[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 62325Isobutyryl chlorideHCID 89728Aminoacetaldehyde dimethyl acetal

Product 1

HCID 22034976HCID 22034976, compoundYield 77%

Procedure

The product is prepared analogously to Example 1 from isobutyryl chloride and aminoacetaldehyde dimethyl acetal. Distillation at 98° C. and 0.01 mbar gives a yield of 77%. According to GC, the product has a purity of 98%.

Workup

  1. distillationDistillation at 98° C.
  2. custom0.01 mbar gives a yield of 77%

Sources & evidence

ORD record
ord-649a3a20f67e409fb2c4de54c66dda1c
Source dataset
uspto-grants-1999_08
Patent number
US05932674

Reaction notes

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